Seismic and ultrasonic frequency measurements on partially saturated rocks under X-ray

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Summary Low-frequency laboratory measurements provide direct access to the elastic properties of samples within the seismic frequency band, offering calibration data for seismic survey analysis. Additionally, µCT imaging can quantify actual saturations and provides insights into phase distributions at the pore scale. To conduct laboratory triaxial measurements at seismic frequencies while simultaneously imaging the rock interior, we developed an X-ray transparent low-frequency apparatus. Our apparatus determines rock mechanical properties at seismic frequencies (0.5–150 Hz) and strain amplitudes (10−7–10−5), measuring Young’s modulus, Poisson’s ratio, and attenuation. In addition P- and S-wave velocities at ultrasonic frequencies are measured. We conducted imbibition-drainage experiments to assess the effect of saturation and patch size on seismic and ultrasonic elastic properties in sandstone. Additional tests with liquid and gaseous CO2 reveal the impact of partial CO2-gas saturation. The imbibition-drainage experiment demonstrated that P-wave velocity at ultrasonic frequencies was elevated during drainage and reduced during imbibition. Drainage caused patchy saturation, while imbibition resulted in uniform saturation. This implies that ultrasonic measurements, with wavelengths comparable to the pore fluid patch size, are likely influenced by scattering. In contrast, low-frequency measurements, where the wavelength surpasses the patch size, capture effective medium properties and therefore are not affected by scattering effects. The results of the CO2 test suggest that low-frequency measurements can detect even low gas saturations (4% gaseous CO2). In contrast, ultrasonic velocity measurements primarily reflect the response of the fully saturated sample at low gas saturations and do not indicate a reduction in velocity. Identifying fluid-solid interactions and estimating saturation via µCT imaging is crucial, especially with minimal gas presence. Our combined approach allows precise determination of elastic properties at seismic frequencies and shows the importance of low-frequency over ultrasonic measurements.