Abstract
The reaction between [PdCl2(PhCN)2] and [Ph2P(S)NH]2CO (H2L) proceeds with monodeprotonation of an amine group in the disulfide ligand to give [Pd(HL)Cl] 1, in which the (HL)− anion supplies an S,N,S′ donor set to palladium(II), leading to disparate S,N chelate ring sizes at the metal.
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