Abstract
Regio- and stereo-selective formation of bicyclo 2-siloxy-2-alkoxyoxetanes 7, 13, 14 was achieved by the proper choice of the solvent and the silyl group in the photoreaction of the cyclic ketene silyl acetals 6, 11, 12 with 2-naphthaldehyde 2, and their transformation to the aldol-type adducts 9, 15, 16 was easily accomplished under the neutral conditions.
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