Abstract
The parameters for the structure of K2Cr2O7 have been refined from 7511 observed reflections; ao = 7.4200(6)Å, bo = 13.399(3)Å, co = 7.3845(9)Å, cosα = −0.1396(2) (α = 98°2'), cosβ = −0.0154(2) (β = 90°53'), cosγ = −0.1078(2) (γ = 96°11'). The discrepancy factor R(Fo2) = 0.0702 with a type 2 extinction correction. The average CrO distances are 1.609Å (unshared) and 1.783Å (shared).
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