Abstract
It was shown that the action of heat on rhodium(III) trifluoroacetate with norbornadiene (NBD) leads to its reduction and the formation of red crystals of [Rh(CF3COO)NBD]2. The formation of the complex was confirmed by elemental analysis and IR, electronic, and x-ray photoelectron spectra. The reaction shows that Rh-Rh compounds can disproportionate under the influence of NBD with the formation of Rh(I) and Rh(III).
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Schedule a callMore From: Bulletin of the Russian Academy of Sciences, Division of chemical science
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