Abstract

The precise use of an electrocatalyst for the HER reaction mainly depends on synthesis cost, durability, and over potential. Recently there is promising research for electrocatalyst synthesis using first-row transition metals. Working towards this herein we present synthesis, physio-chemical characterization, and hydrogen evolution activity of amino guanidium metal naphthoate complexes. The obtained electrocatalysts were characterized by element analysis, IR spectra, UV-Visible spectroscopy, TG-DTA, and powder-XRD. The thermal behavior of these compounds has been studied by simultaneous TG-DTA techniques. The isomorphic nature of the metal complexes is evident from powder-XRD data.

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