Abstract
By the use of pulse cyclic chronovoltammetry, better analytical data are sometimes obtained during the reverse scans. This is demonstrated by a chronovoltammetric FIA study of the quinone–hydroquinone couple. A quantitative FIA pulse cyclic chronovoltammetric investigation of the ferri–ferrocyanide reversible couple showed linearity for time-integrated fourier-smoothed data for reduction scan currents as well as the total of the forward and reverse scan peak currents. The detection limit was found to be 2 × 10−6 M.
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