Abstract

A thermal oxide patterning method has proven to be effective for correcting coating-stress-induced distortion on flat silicon wafers. We report progress on developing this method for correcting curved silicon mirrors distorted by front-side iridium coatings. Owing to the difference in geometry, a finite element model has been established to calculate the appropriate duty cycle maps in thermal oxide hexagon patterns used for compensation. In addition, a photolithographic process, along with three-dimensional printed equipment, has been developed for creating patterns precisely on the back side of curved mirrors. The developed method has been used to recover the original surface shape of two silicon mirrors which are 100-mm long, 0.5-mm thick, having 312-mm radius of curvature, and 30 deg in azimuthal span (Wolter-I geometry). These mirrors’ front sides are sputter-coated by 20-nm iridium layers with ∼-70 N / m integrated stress. Measurement results show that the developed method can mitigate coating-induced distortion by a factor of ∼5 in RMS height and ∼4 in RMS slope error, corresponding to ∼0.5 arc sec RMS slope error. Residual errors after correction are dominated by mid-frequency ripples created during the annealing process, which will be resolved in the future. The presented method is precise and inexpensive and a potential candidate for resolving the coating stress issue for Lynx optics in the future.

Highlights

  • NASA’s next-generation flagship x-ray telescope concept, called Lynx, is currently under study for consideration by the 2020 Astrophysics Decadal Review.[1]

  • The process was applied to two mirrors, 312S1024 and 312P1052, to compensate for the surface distortion induced by 20-nm iridium coatings

  • We have developed a thermal oxide patterning method for compensating silicon mirror distortion induced by coating stress

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Summary

Introduction

NASA’s next-generation flagship x-ray telescope concept, called Lynx, is currently under study for consideration by the 2020 Astrophysics Decadal Review.[1]. Space Flight Center, by measuring the wafer curvature in situ and controlling the working gas pressure, was able to deposit a 15-nm-thick iridium layer on a 2-inch diameter flat wafer with stress around 3 MPa (0.05 N∕m),[7] which may be low enough for Lynx.[8] the coating stress uniformity, stability, and reflectivity are critical and have not yet been demonstrated Another group at GSFC tried to balance the compressive stress in iridium films by depositing a chromium layer with tensile stress underneath the iridium.[9] They attempted to reduce the compressive stress in iridium layers by annealing at 350°C.6. We report progress of extending this method to GSFC’s curved silicon mirrors

Process
Metrology and Stress Calculation
Pattern Design
Photo Lithography Process on Curved Mirrors
Results
Conclusions

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