Abstract
The thermal insulation performance of intumescent coating coated on the surface of steel structure is of great significance to prevent the underlying steel structure from collapse in fire. Bio-based intumescent flame retardants gradually attract many attentions due to its environmental friendliness and rich natural sources. In this study, a new bio-based intumescent flame retardant trinity lignin intumescent flame retardant (TLI) is synthesized, which is added to epoxy resin (EP) to prepare EP/TLI epoxy intumescent coatings. The burning behavior of EP/TLI epoxy intumescent coatings is investigated by thermogravimetric (TG) analysis, limit oxygen index (LOI), vertical burning test and cone calorimeter test. Microscopic morphology of char layer is observed by scanning electron microscopy (SEM). The results show that when the TLI addition content is 20 wt% (EP/TLI-4), LOI reaches 26.5 %, UL-94 is V-0 rating. Compared to pure EP, the peak heat release rate (pHRR) and total heat release (THR) of EP/TLI-4 coating are reduced by 82.20 % and 78.27 %, respectively. The influence of chemical formulations, initial coating thickness and incident heat flux on heat transfer process of EP/TLI epoxy intumescent coatings is also investigated. At the same time, the thermal insulation mechanism of EP/TLI epoxy intumescent coating is presented.
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