Abstract
Tris(fluorosulphato)vanadium(III) has been synthesised by interacting vanadium(III) chloride and fluorosulphuric acid. Its complexes with pyridine, ethylenediamine and triphenylphosphine oxide have also been isolated. In all these complexes, the infrared spectra suggest the lower symmetry of fluorosulphate groups and the magnetic moment values are in close proximity for a d 2 system. The reflectance spectra reveal the hexacoordination around vanadium(III). Thermal analysis corresponds to four steps decomposition for tris(fluorosulphato)vanadium(III).
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