Abstract
In this paper, NiCo2S4 nanoelectrode materials were prepared by a two-step hydrothermal method. Physical and morphological characterization and electrochemical testing revealed that the prepared NiCo2S4 has a sea urchin-like layered three-dimensional network structure, which can fully increase the contact area with the electrolyte, increase the active sites and improve the electrochemical performance. The specific capacitance of the prepared NiCo2S4 nanomaterials reached 717.32 F/g. The cyclic voltammetry test curve as well as galvanostatic charge-discharge (GCD) test curve have perfect symmetry, good material reversibility. Electrochemical impedance spectroscopy (EIS) indicates materials with low impedance. The specific capacitance remained 76.8% after 3000 cycles and the electrochemical stability was good. NiCo2S4 electrode material has excellent electrochemical properties and has a promising application in supercapacitor electrodes.
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