Abstract
Synthesis of copper oxide (CuO) nanorods was achieved by thermal decomposition of the precursor of CuC 2O 4 obtained via chemical reaction between Cu(CH 3COO) 2·H 2O and H 2C 2O 4·2H 2O in the presence of surfactant nonyl phenyl ether (9)/(5) (NP-9/5) and NaCl flux. Transmission electron microscopy (TEM), X-ray diffraction (XRD), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), selected-area electron diffraction (SAED) and high-resolution TEM (HRTEM) were used to characterize the structure features and chemical compositions of the as-made nanorods. The results showed that the as-prepared nanorods is composed of CuO with diameter of 30–100 nm, and lengths ranging from 1 to 3 μm. The mechanism of formation of CuO nanorods was also discussed.
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