Abstract

Electron beam melting (EBM) is a powder bed additive manufacturing process where a powder material is melted selectively in a layer-by-layer approach using an electron beam. EBM has some unique features during the manufacture of components with high-performance superalloys that are commonly used in gas turbines such as Alloy 718. EBM has a high deposition rate due to its high beam energy and speed, comparatively low residual stresses, and limited problems with oxidation. However, due to the layer-by-layer melting approach and high powder bed temperature, the as-built EBM Alloy 718 exhibits a microstructural gradient starting from the top of the sample. In this study, we conducted modeling to obtain a deeper understanding of microstructural development during EBM and the homogenization that occurs during manufacturing with Alloy 718. A multicomponent phase-field modeling approach was combined with transformation kinetic modeling to predict the microstructural gradient and the results were compared with experimental observations. In particular, we investigated the segregation of elements during solidification and the subsequent “in situ” homogenization heat treatment at the elevated powder bed temperature. The predicted elemental composition was then used for thermodynamic modeling to predict the changes in the continuous cooling transformation and time–temperature transformation diagrams for Alloy 718, which helped to explain the observed phase evolution within the microstructure. The results indicate that the proposed approach can be employed as a valuable tool for understanding processes and for process development, including post-heat treatments.

Highlights

  • RECENTLY, powder bed additive manufacturing (AM) has attracted great interest from the manufacturing industries and research community because of its capacity to produce near net shape structures with complex geometries, which cannot be manufacturedManuscript submitted November 21, 2018

  • We modeled the microstructure using the multiphase-field method and the transformation kinetics were determined to understand the formation of the microstructural gradient in Alloy 718 samples produced using electron beam melting (EBM)

  • These particles were confirmed as the Laves phase and NbC/(Nb,Ti)(C,N) according to transmission electron microscopy (TEM) analysis

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Summary

INTRODUCTION

RECENTLY, powder bed additive manufacturing (AM) has attracted great interest from the manufacturing industries and research community because of its capacity to produce near net shape structures with complex geometries, which cannot be manufactured. Nickel-based superalloys are among the most important alloys used in aerospace applications and gas turbine engines because of their high-temperature strength, high resistance to creep deformation, and corrosion resistance.[2,3] Among these superalloys, Alloy 718 is one of the most widely used nickel-iron-based superalloys and it is suitable for AM processes because of its good weldability due to the sluggish precipitation of the main strengthening phase c¢¢.[4] The microstructure of Alloy 718 is dominated by an austenitic c fcc matrix. As the subsequent layers are built, the solidified structure gradually undergoes ‘‘in situ’’ heat treatment due to the elevated powder bed temperature (> 1000 °C for Alloy 718) in the EBM process.

EXPERIMENTAL
MICRESS and the Governing Equation
Model Setup in MICRESS and Assumptions
Experimental Results: ‘‘In Situ’’ Homogenization and Phase Formation
Homogenization Behavior of EBM Alloy 718 and Cast Alloy 718
Change in Precipitation Kinetics of Phases in the Microstructure
CONCLUSION
Steinbach
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