Post-irradiation annealing effects on microstructure and helium bubbles in neutron irradiated type 304 stainless steel

Abstract

Helium bubble nucleation and growth processes were studied at elevated temperatures on type 304 stainless steel which had been neutron irradiated to 1.4 × 1026 n/ m 2 ( E > 1 MeV) and annealed at 400, 550, 650 and 900°C for 1 h. After annealing, specimens for microstructural observation were prepared and observed (by transmission electron microscope (TEM).) Radiation defects were present at high density in the as-irradiated specimens and annealed out with increasing annealing temperature. Helium bubbles became visible where defects were annealed out (above 650°C). The bubbles grew preferentially at dislocations and grain boundaries. At the grain boundaries, most of the helium bubbles formed on grain boundary dislocations. It was concluded that during post-irradiation annealing, the dislocations which remained after annealing played an important role in helium bubble growth, even in the grain boundaries.