Abstract
Abstract Photoinduced‐addition of methanol to (5S)‐(5‐O‐tert‐butyldimethylsiloxymethyl)furan‐2(5H)‐one: (4R,5S)‐4‐hydroxymethyl‐(5‐O‐tert‐butyldimethylsiloxymethyl)furan‐2(5H)‐one intermediate: methyl (4S)‐4,5‐O‐isopropylidenepent‐(2Z)‐enoate intermediate: (S)‐5‐hydroxymethylfuran‐2(5H)‐one intermediate: (5S)‐(5‐O‐tert‐butyldimethylsiloxymethyl)furan‐2(5H)‐one product: (4R,5S)‐4‐Hydroxymethyl‐(5‐O‐tert‐butyldimethylsiloxymethyl)furan‐2(5H)‐one reactant: 23.7 g (0.13 mol) of benzophenone byproduct: benzpinacol byproduct: (4R,5S)‐4‐diphenylhydroxymethyl‐5‐tert‐butyldimethylsiloxymethylfuran‐2(5H)‐one
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