Abstract
Tetrahydrofuran can be produced from agricultural waste rich in pentosans such as corn stalks. The furan hydrogenation reaction was carried out in the presence of charcoal-supported catalysts, without a solvent, under constant hydrogen pressure. Determination of the principal effects and the effects of interaction of the factors likely to influence the reaction can be achieved through a full two-level factorial design. Interpretation of the results obtained allows the choice of a new experimental mode, corresponding to milder operating conditions. Optimization of the conditions for the production of tetrahydrofuran was carried out with a Doehlert experimental matrix. A study of the corresponding response surfaces shows that high yield can be obtained at low pressure and with a reduced quantity of catalyst.
Published Version
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