Abstract
Ni(C6HsN202) 2.10.5, tetragonal, P4/mcc, a= 15553(4), c= 6.307(3) ./~, Z= 4. The structure has been determined by standard methods from single-crystal X-ray diffractometer data and refined by least-squares methods to R=0.095 for 725 independent reflexions. The metal-complex units form columnar stacks with Ni-Ni distances of 3.153(3) A. Iodine chains run parallel to the stacks.
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