Abstract
Under biphasic conditions (CH 2 Cl 2 /H 2 O) using acetone, oxone, buffer and phase-transfer catalyst Bu 4 NHSO 4 (su−), some secondary amines without α hydrogens are oxidized to their corresponding nitroxides in rapid and good yields. Under biphasic conditions (CH 2 Cl 2 /H 2 O) using acetone, oxone, buffer and phase-transfer catalyst Bu4NHSO 4 , some secondary amines without α hydrogens are oxidized to their corresponding nitroxides in rapid and good yields (75–93 %).
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