Abstract
A simple azabicyclic peroxide synthesis was achieved by the manganese(III)-mediated oxidative formal [2+2+2] cycloaddition. A mixture of tetramic acid derivatives and alkenes was oxidized with manganese(III) acetate under a dry air stream to give 1-hydroxy-8-aza-2,3-dioxabicyclo[4.3.0]nonan-7-ones in good to quantitative chemical yields.
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