Abstract
An efficient method has been developed for the synthesis of <i>C</i>-glycosyl amino acids through a tandem nucleophilic opening–cyclization of an <sc>l</sc>-<i>ido</i>-bisepoxide with the anion of Schöllkopf’s bislactim. A masked amine was introduced at the CH<sub>2</sub>C<sub>1</sub>-position of the resulting compound. The products are enantiopure polyfunctionalized intermediates, suitable for further synthesis of antibacterial compounds.
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