Abstract
The X-ray diffraction study of a new heterometallic cluster CpReFePt(μ3-C=CHPh)(CO)5[P(OPri)3]2 is performed. The crystallographic characteristics are as follows: a = 11.0275(4) A, b = 33.0367(12) A, c = 12.2691(5) A, β = 98.3660(10)°, V = 4422.2(3) A3, space group P21/n, Z = 4, dcalc = 1.744 g/cm3. The cluster contains the phenylvinylidene ligand coordinated with a trimetallic core in the form of a Re–Fe–Pt chain (the Re–Fe and Fe–Pt bond lengths are 2.794(7) A and 2.628(1) A respectively; the Re···Pt distance is 3.354(1) A).
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