Abstract
A new method for preparation of alkaline molybdenum bronzes using molybdate crystalline hydrate precursor was elaborated. The reaction products contain sodium hydroxide and sodium molybdenum oxide bronzes Na x MoO 3. The bronzes were characterized by X-ray diffraction and electron microscopy. The dimensions of Na x MoO 3 are non-uniform: nanosized Na x MoO 3 ( x=0.03–0.08, MoO 3 structure type) and micrometer sized cubic Na x MoO 3 ( x=0.33–0.92) particles were obtained.
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