Abstract
[100-75-4] C5H10N2O (MW 114.15) InChI = 1S/C5H10N2O/c8-6-7-4-2-1-3-5-7/h1-5H2 InChIKey = UWSDONTXWQOZFN-UHFFFAOYSA-N (a precursor to piperidine radical cation and nitroso radical species) Alternative Names: 1-nitrosopiperidine; NPI; NPIP. Physical Data: bp 219 °C; density 1.0631 g cm−3 (at 18.5 °C). Solubility: sol in most organic solvents (CHCl3, EtOAc, THF, MeOH). Form Supplied in: yellowish oil. Preparative Methods: nitrosation of piperidine using NaNO2 in acidic conditions or tert-butyl nitrite (t-BuONO) under neutral conditions. Purification: flash column chromatography on silica gel, eluted with 10% EtOAc in hexanes. Handling, Storage, and Precautions: a known carcinogenic compound; should be handled with care; can be stored under inert atmosphere at <4 °C.
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