Abstract
The molecule of the title compound, C22H27NO9, an azasugar derivative, consists of one benzene ring and two fused rings, which have the cis arrangement at the ring junctions, and gives a V-shaped geometry. The interplanar angle between the five- and six-membered rings is 65.69 (11)°. The crystal structure is stablized by weak intermolecular C—H⋯O hydrogen bonds.
Highlights
The molecule of the title compound, C22H27NO9, an azasugar derivative, consists of one benzene ring and two fused rings, which have the cis arrangement at the ring junctions, and gives a V-shaped geometry
As a contribution to the azasugars chemistry, we report here the crystal structure of the title compound, which was obtained under one-pot reaction (Sachin et al, 2004 and Saito et al, 2002) of N-benzyl-6-deoxy- 3,6-imino-methylene-1,2-O-isopropylidene-α-D-allofuranose
The oily was recrystallized from methanol to give the title compound as a white crystal
Summary
R factor = 0.043; wR factor = 0.107; data-to-parameter ratio = 8.6. The molecule of the title compound, C22H27NO9, an azasugar derivative, consists of one benzene ring and two fused rings, which have the cis arrangement at the ring junctions, and gives a V-shaped geometry. The interplanar angle between the fiveand six-membered rings is 65.69 (11). The crystal structure is stablized by weak intermolecular C—H O hydrogen bonds
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More From: Acta Crystallographica Section E Structure Reports Online
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