Abstract
In the title compound, C19H13Br2NO, the dihedral angle between the rings of the biphenyl group is 53.59 (14)°. The ring of the benzamide group is inclined to the phenyl rings of the biphenyl group by 23.87 (15) and 75.89 (15)°. There are no significant intermolecular interactions in the crystal structure.
Highlights
In the title compound, C19H13Br2NO, the dihedral angle between the rings of the biphenyl group is 53.59 (14)
The ring of the benzamide group is inclined to the phenyl rings of the biphenyl group by 23.87 (15) and 75.89 (15)
As part of our studies on the substituent effects on the structures and other aspects of dibromo biphenyl derivatives, 4,4′-Dibromo-2nitrobiphenyl (Novina et al, 2012), in the present work we report on the synthesis and crystal structure of the title compound
Summary
R factor = 0.033; wR factor = 0.075; data-to-parameter ratio = 16.6. C19H13Br2NO, the dihedral angle between the rings of the biphenyl group is 53.59 (14). The ring of the benzamide group is inclined to the phenyl rings of the biphenyl group by 23.87 (15) and 75.89 (15). There are no significant intermolecular interactions in the crystal structure. Data collection: APEX2 (Bruker, 2004); cell refinement: APEX2 and SAINT (Bruker, 2004); data reduction: SAINT and XPREP (Bruker, 2004); program(s) used to solve structure: SHELXS97. (Sheldrick, 2008); molecular graphics: ORTEP-3 (Farrugia, 2012); software used to prepare material for publication: PLATON (Spek, 2009)
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