Abstract

X-ray microscopy at photon energies above 15 keV is very attractive for the investigation of atomic and nanoscale properties of technologically relevant structural and bio materials. This method is limited by the quality of X-ray optics. Multilayer Laue lenses (MLLs) have the potential to make a major impact in this field because, as compared to other X-ray optics, they become more efficient and effective with increasing photon energy. In this work, MLLs were utilized with hard X-rays at photon energies up to 34.5 keV. The design, fabrication, and performance of these lenses are presented, and their application in several imaging configurations is described. In particular, two "full field" modes of imaging were explored, which provide various contrast modalities that are useful for materials characterisation. These include point projection imaging (or Gabor holography) for phase contrast imaging and direct imaging with both bright-field and dark-field illumination. With high-efficiency MLLs, such modes offer rapid data collection as compared with scanning methods as well as a large field of views.

Highlights

  • Hard X rays with photon energies in the range of 15 keV to over 100 keV can be used to investigate the structures of materials for a wide range of applications [1, 2]

  • Multilayer Laue lenses (MLLs) have the potential to make a major impact in this field because, as compared to other X-ray optics, they become more efficient and effective with increasing photon energy

  • The two MLLs must be optimized for the same photon energy but manufactured with focal lengths whose difference is equal to the separation of the lenses, so that they focus in both directions to a common point

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Summary

Introduction

Hard X rays with photon energies in the range of 15 keV to over 100 keV can be used to investigate the structures of materials for a wide range of applications [1, 2]. By mapping the structure of deeply-embedded crystalline elements in three dimensions at nanometer resolution one would be able to determine the influence of domain walls or defects on macroscale mechanical or physical structural properties, for example This requires wavelengths short enough to Bragg-reflect from lattices of the material, combined with an imaging methodology to localise the origin of scattering. This includes the analysis of the wavefronts of individual lenses, 2D focus analysis, and presentation of full field microscopy images obtained with these sets of lenses. The final section focuses on full field imaging and the future perspective is briefly outlined

MLL fabrication and operation
D Number NA
Experimental setup
Imaging geometries
Projection holography with a real source
Projection holography with a virtual source
Direct imaging
Basic performance of the MLLs
Wavefront characterization and resolution
Diffraction efficiency
Demonstration of direct imaging
Findings
Conclusions
Full Text
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