Abstract
New developments in high-resolution multidimensional NMR of solids are described. Special emphasis is placed on double-quantum (DQ) methods employing fast magic angle spinning (MAS). This new technique allows structural elucidation with atomistic resolution including hydrogen positions in non-crystalline materials and the determination of the anisotropy of chain motions by probing residual dipolar couplings between adjacent groups along a macromolecule. Specific examples include hydrogen bonded systems, columnar structures with π-π interactions, polymer melts and block copolymers.
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