Abstract

In the present study, a coarse-grained Cu–0.5 wt% Zr alloy was repeatedly processed by a novel technique of rotational constrained bending (RCB). In this technique, the workpiece was deformed by bending in a channel with an angle of 90°, using a rotating roller. The influence of the number of passes (N) of RCB on strain distribution, microstructure evolution and mechanical properties of the alloy was investigated. The heterogeneous distribution of the microhardness in the billet cross-section after the first pass was transformed into a homogeneous one after twelve passes, due to the rotation of the sample by 90° clockwise between individual passes. In addition, the gradual refinement/homogenization of the microstructure and formation of strong (110) crystallographic texture were found with increasing N. The initial grain size of 180 μm decreased down to 3.4 μm after twelve passes. The dislocation density increased by two orders of magnitude after RCB processing. In accordance with the grain-size refinement and the strong increase of the dislocation density, RCB processing significantly enhanced the strength of the alloy, while the ductility considerably decreased. The yield stress increased from 63 to 524 MPa, while the elongation to failure decreased below 10% after twelve passes.

Highlights

  • Utilization of severe plastic deformation (SPD) techniques for processing of metallic materials was found to be effective in substantial microstructure refinement and enhancement of mechanical properties [1,2,3,4,5]

  • A scanning electron microscopy (SEM) micrograph and a grain orientation map for the initial state of Cu–0.5 wt% Zr alloy are shown in Figure 2a,b, respectively

  • Comprehensive microstructure characterization in the central part of the cross-section was performed by the combination of scanning electron microscopy (SEM) and electron and X-ray diffraction

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Summary

Introduction

Utilization of severe plastic deformation (SPD) techniques for processing of metallic materials was found to be effective in substantial microstructure refinement and enhancement of mechanical properties [1,2,3,4,5]. Equal channel angular pressing (ECAP) [6,7,8] and high-pressure torsion (HPT) processes [9,10,11] have been considered as the most popular and widely applied SPD methods so far These techniques impose shear deformation on the workpieces during processing of the samples in special dies, preserving the original dimension and shape of the samples. The material is processed through the set of rollers, which significantly reduce the friction forces acting during the processing and allow for the processing of long billets at higher speeds, as in the case of the other SPD methods This concept was employed for the development of a newly designed constrained bending die, consisting of one driven roller in the top part of the bended channel with a uniform cross-section. FFiigguurere1.1(a.)(Sac)hSemchateicmoaf tthice odifetfhorepdroiecefsosirngpvroiacceosnssitnraginvediabecnodninsgtr. aTihneemdabinepnadrtinofgt.heTdhiee main part of the die ccoommpprisreisse1s—1p—lunpgleur,n2g—ebr,il2le—t, 3b—ilrloeltle,r3a—ndr4o—llestreealnddie.4(—b) Ostreieenltadtiioen. (obf t)hOe wrioernktpaietcioe nin othfethe workpiece in the omorretthnhotsog.ognoanl acolocrodoinradteinsyastteemsyussteedmforurseepdrefsoenrtarteiopnreosfemnictarothioarndnoefsms aincdrotehxaturrdenmeesassuarned- texture measurements

Microstructure of the Initial Sample and the Specimen Processed by One Pass
Evolution of the Microstructure with Increasing Number of Passes
Conclusions
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