Abstract

Solidification of an aqueous solution was studied using a laser interferometry technique combined with an optical microscope. In order to measure the concentration distribution in an aqueous NaCl solution near an ice crystal and the three-dimensional shape of the ice crystal in a known temperature field, a directional solidification stage was used. This was composed of low- and high-temperature blocks and a moving bed. In our experiment, ice crystals showed four shapes: flat, treelike, swordlike, and needlelike. As a result of the interferometry experiment, it was observed that the concentration increases in the bulk solution for thick samples, swordlike ice crystals have an asymmetric triangular cross section, and treelike crystals have a flat and low top. We also studied ice formation response to injection of a high-concentration solution. © 1998 Scripta Technica, Heat Trans Jpn Res, 27(5): 353–364, 1998

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