Abstract
High temperature brazing of nickel-based superalloys often produces joints containing hard, brittle micro-constituents that can be detrimental to mechanical properties and challenging to characterise consistently. In this study, techniques including low angle micro-sectioning, image analysis with ImageJ and electron probe micro-analysis were used to determine the composition, hardness and dispersion parameters of phases in single crystal superalloy CMSX-4, vacuum furnace brazed with BNi-2 and BNi-9 filler metals (FMs). Both FMs produced similar joints with hard centreline eutectic phases, a soft isothermally solidified zone and boron diffusion-affected zone in the CMSX-4. The volume fraction, particle size distribution and inter-particle spacing data generated will provide a framework for future metallurgical characterisations and assist in the development of microstructure–mechanical property relationships.
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