Mechanism of microstructure and texture evolution during hot rolling of pure Mg and Mg-0.2%Ce alloy

Abstract

ABSTRACT The extruded samples of pure Mg and Mg-0.2%Ce alloy were subjected to a 90% reduction in thickness at 250°C during hot rolling. The microstructure, texture, and mechanical properties of the hot-rolled samples were evaluated. The microstructural evolution shows the presence of shear bands in Mg-0.2%Ce alloy at an angle of 30-35° concerning the normal direction and no such bands are observed in pure Mg. Upon annealing the samples at 400°C for one hour, it is observed that the grain size of Mg-0.2%Ce is smaller than pure Mg indicating that the precipitates of Ce arrest grain boundary mobility. The ex-situ EBSD microstructure analysis results show a higher change in the value of α33 components after annealing for pure Mg compared to Mg-0.2%Ce alloy suggesting the precipitates of Mg12Ce stabilises the pyr. <c + a > dislocations. The basal texture is observed in both samples after hot rolling. The experimental texture was simulated using the visco-plastic self-consistent (VPSC) modelling where it is observed that the initial extruded texture is favourable for the higher activity of pyr. <c + a > dislocation and extension twinning in Mg-0.2% e alloy. Further, the yield locus shows that Mg-0.2%Ce alloy shows relatively lower anisotropy compared to pure Mg. The yield strength and UTS of the pure Mg are higher than the Mg-0.2%Ce alloy which is attributed to the relatively more dislocation-dislocation interaction in pure Mg compared to Mg-0.2%Ce alloy resulting in the lower mean free path of the dislocations in pure Mg.