Abstract

We report on the magnetization and high-frequency EMR studies of lithium manganese spinel LiMn2O4 powder samples obtained by the sol–gel method with calcinations at several temperature ranges. The results indicate that the low temperature magnetization and EMR spectra vary strongly between samples. Analysis of the experimental data enables a deeper characterization of the samples. It appears that a small amount of the impurity phase Li2MnO3 exists in the samples obtained by calcinations at 900°C.

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