Abstract
The application of non‐toxic and magnetically separable nano‐CuFe2O4 as an efficient catalyst for oxidative homo‐ and cross‐coupling reaction of terminal alkynes is described. A wide range of symmetrical and unsymmetrical 1,3‐diynes have been synthesized in moderate to good yields under ambient atmosphere. The nano CuFe2O4 can be recovered with a magnet and reused at least five consecutive cycles with no appreciable loss of its catalytic activity.
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