Abstract

AbstractRoll/slide friction tests were carried out at a temperature of 750°C in a vacuum. Disc specimens were made of Si3N4 with or without a sputtered MoS2 film. A pin specimen was rubbed against one disc to supply a lubricating transfer film. With a pin made of an MoS2‐based composite, the friction coefficient was around 0.3 and almost no wear of the discs was observed after 24 h of operation at a load of 50 N, a rotating speed of 0.5 m/s, and a slip ratio of 10%. Transferred patchy MoS2 films were observed on the friction track. With a pin made of Ni‐based composite containing BN and graphite, the friction coefficient increased from 0.2 to 0.7 over a test time of about 8 h and severe disc wear was found. In an additional test using Si3N4 discs with a sputtered MoS2 film without a pin, the friction coefficient was about 0.3, and no wear of the discs was found after 24 h of operation. The appearance of the friction track was similar to that in the test using the MoS2‐based composite pin. It seems that the sputtered MoS2 film wore, but wear particles reattached on the friction path to develop an effective lubricating film. These results demonstrate the effectiveness of transfer film lubrication for long‐term operation in a high‐temperature vacuum, and the superior ability of MoS2 to develop an effective transfer film.

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