Abstract
Bulk and nano-sized NbTi(PO4)3 has been prepared by citrate gel pyrolysis using peroxo titanium complex as one of the reactants, and ethylene glycol as gelating reagent. The compound was analyzed by powder XRD and infrared methods. It is found to crystallize in rhombohedral lattice with space group . The infrared spectra of samples prepared at different temperatures consist of mainly bands due to phosphate (PO4) group. The morphological characterization was carried out by transmission electron microscopy. The crystallite size was estimated from the line width of intense powder diffraction line using Scherrer's formula and TEM images.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callMore From: Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry
Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
