Abstract
AbstractThe epoxidation of allylic compounds: allyl alcohol, methallyl alcohol and methallyl chloride to corresponding epoxides: glycidol, 2-methylglycidol and 2-methylepichlorohydrin with hydrogen peroxide over Ti-MCM-48 catalyst has been studied. The epoxidation was carried out with 30 wt% hydrogen peroxide in methanol as a solvent under autogenic pressure (in autoclave) and at atmospheric pressure in a glass reactor. The optimal technological parameters and regions of advantageous changes of: temperature, the molar ratio allylic compound/H
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