Abstract
Three new proline (pro) lead(II) complexes were synthesized and characterized by elemental analyses, IR, 1H NMR, and 13C NMR spectroscopy. Single crystal X-ray structural analysis of [Pb(pro)(H2O)] n shows the complex to be a novel 1D chain polymer as a result of water bridging. Coordination number of Pb(II) is six, with a ‘stereo-chemically active’ electron lone pair, and the coordination sphere is hemidirected. The chains interact with each other via weak Pb ··· O intractions and hydrogen bonding to create a 2D framework.
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