Abstract
The intercalates of unhydrated VOSO 4 and VOPO 4 with alcohols (C 1 to C 8) have been prepared and characterized by their compositions, basal spacings and thermal stabilities. X-ray powder studies show that the layered structures of VOSO 4 and VOPO 4 lattices are maintained in these complexes. The alcohol molecules are penetrated into van der Waal's gaps of the host lattices and form bimolecular layers. The observed alternation of the basal spacing increments with the number of carbon atoms of the linear aliphatic chain is explained from the arrangement of these chains.
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