Abstract
ABSTRACT0.6PMN-0.4PZN solid solution ceramic was synthesized employing two stage columbite route using sintering temperature range 1000–1170°C for calcination temperature 800°C and 850°C respectively. XRD and SEM characterization revealed single perovskite phase formation in ceramic between 1050°C to 1100°C. The highest density upto 94% was achieved for the composition under study. The excellent dielectric properties were obtained at lower sintering temperature 1000–1100°C. Ceramics sintered between 1000°C-1100°C exhibit ϵmax≈14000 and 24000 at 1 kHz with Tc = 51–48°C which is near room temperature. A good correlation was obtained between dielectric properties with structure, microstructure and density. The TCC values within the limit of Z5U capacitor specification reflect ceramics of composition 0.6PMN-0.4PZN is a potential candidate for MLC.
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