Koenigs–Knorr reaction of fusel alcohols with methyl (1-bromo-2,3,4-tri-O-acetyl-α-d-glucopyranosid)uronate leading to the protected alkyl glucuronides—crystal structures and high resolution 1H and 13C NMR data

Bettina Mönch,Antje Gebert,Franziska Emmerling,Roland Becker,Irene Nehls

doi:10.1016/j.carres.2012.01.002

Koenigs–Knorr reaction of fusel alcohols with methyl (1-bromo-2,3,4-tri-O-acetyl-α-d-glucopyranosid)uronate leading to the protected alkyl glucuronides—crystal structures and high resolution 1H and 13C NMR data

Bettina Mönch, Antje Gebert + Show 3 more

https://doi.org/10.1016/j.carres.2012.01.002

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Journal: Carbohydrate research	Publication Date: Jan 13, 2012
Citations: 13

Affiliation: Federal Institute For Materials Research and Testing

#High Resolution 1H #High Resolution 13C NMR + Show 8 more

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Abstract

Crystal structures and high resolution 1H and 13C NMR spectral data for methyl (alkyl 2,3,4-tri-O-acetyl-β-d-glucopyranosid)uronates (alkyl=methyl, ethyl, n-propyl, i-propyl, n-butyl, sec-butyl, i-butyl, n-pentyl, 2-methyl-1-butyl and 3-methyl-1-butyl) are presented.

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