Abstract

Thermogravimetry (TG) and electron microscopy (EM) methods were used to study the isothermal dehydration of Na 3P 3O 9·6H 2O single crystals and polycrystalline samples in flowing nitrogen at 35–60°C. The effect of granulometry on the kinetic characteristics of reversible dehydration, which under conditions of uniform localization proceeds with an induction period, self-acceleration and deceleration, was studied.

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