Abstract
The bromide released by the alkaline hydrolysis of N-bromosuccinimide and its reactions with bromide, pyridoxine and thiamine have been studied potentiometrically using a solid-state bromide-selective electrode to monitor the consumed or produced bromide ion. Potential—time indications are obtained using a microcomputer-controlled potentiometric system. The overall rate constants and the activation energies have been calculated. A kinetic—potentiometric procedure for the determination of pyridoxine in the presence of thiamine in pharmaceutical preparations, based on its reaction with N-bromosuccinimide, is presented.
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