Abstract
Samples of YBa2Cu3Ox were prepared by solid state reaction and characterized by resistivity and magnetic measurements, x-ray diffraction, and electron microprobe analysis. The oxygen pressure was measured directly as function of temperature under isochoric conditions with minimized free volume. DTA and in situ x-ray analysis with a high temperature Guinier camera were carried out under the same conditions. H2O, N2 and Co2 were detected as contaminants by mass spectrometry. AT high temperatures the results obtained from the direct measurements agree well with those deduced from isobaric measurements. At low temperatures and pressures the latter yield substantially lower values. This might be due to incomplete equilibration.
Sign-in/Register to access full text options 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
