Abstract

The reduction of cerium IV in hot concentrated sulphuric acid and in sulphuric acid hydrates, respectively, is investigated. It is found that on raising the concentration of sulphuric acid, the degree of reduction also increases. The degree of reduction depends to a great extent on the relative quantities of solid substance weighed and of sulphuric acid used for the boiling treatment. In contrast to other suggested mechanisms, no correlation is found to exist between the gaseous oxygen developed during reduction and the oxygen bound by sulphuric acid.

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