Abstract
Aminophenyl- and pyridinium-substituted porphyrins were intercalated into the α phase of zirconium hydrogen phosphate (α-ZrP) by exchanging the porphyrins into the p-methoxyaniline (PMA) preintercalated compound Zr(O 3 POH) 2 .2PMA (α-ZrP.2PMA). Porphyrin exchange reactions with α-ZrP and its ethanol intercalate were unsuccessful. Powder X-ray diffraction patterns of p-H 2 TAPP- and H 2 TMPyP-exchanged α-ZrP-2PMA revealed complete conversion of the starting material to phases with interlayer spacings near 17 A, corresponding to a guest layer thickness of ca. 11 A
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