Integrating superregenerative principles in a compact, power-efficient NMR/NQR spectrometer: A novel approach with pulsed excitation

Abstract

We present a new approach to Nuclear Quadrupole Resonance (NQR)/Nuclear Magnetic Resonance (NMR) spectroscopy, the Damp-Enhanced Superregenerative Nuclear Spin Analyser (DESSA). This system integrates Superregenerative principles with pulsed sample excitation and detection, offering significant advancements over traditional Super-Regenerative Receivers (SRRs). Our approach overcomes certain limitations associated with traditional Super-Regenerative Receivers (SRRs) by integrating direct digital processing of the oscillator response delay time (Td) and an electronic damp unit to regulate the excitation pulse decay time (Te). The essence is combining pulsed excitation with a reception inspired by, but distinct from, conventional SRRs. The damp unit allows a rapid termination of the oscillation pulse and the initiation of detection within microseconds, and direct digital processing avoids the need for a second lower frequency which is used for quenching in a traditional SRRs, thereby avoiding the formation of sidebands. We demonstrate the effectiveness of DESSA on a NaClO3 sample containing the isotope Chlorine-35 where it accurately detects the NQR signal with sub-kHz resolution.