Abstract
A series of 17 cyano(ligand)cobaloximes have been prepared, including 6 with 4-substituted pyridine ligands, 6 with primary amine ligands, 3 with 4-substituted aniline ligands, the ammonia complex, and the potassium salt of the thiocyanato complex. The analogous series of complexes enriched in 13 C and 15 N in the cyanide ligand have been used to locate the cyanide 13 C and 15 N NMR resonances and the cyanide stretching frequencies in the infrared spectra
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