Abstract
This study examined the stress corrosion cracking (SCC) phenomenon of Alloy 600 in a high-temperature primary water environment. The investigation involved the observation of local plastic deformation and SCC initiation on the specimen surface using an observation apparatus, comprising a laser confocal microscope (LCM) and an autoclave equipped with a diamond window view-port. Prior to conducting the SCC initiation test, the crystalline structure of the specimen, including grain boundary (GB) characteristics, Schmid factor, and trace inclination angle, underwent examination using an electron backscatter diffraction (EBSD) technique. The local strain distribution was subsequently analyzed using a digital image correlation (DIC) method, employing LCM images obtained during the SCC experiments. The ex-situ EBSD analysis indicated that SCC mainly initiated at random high-angle grain boundaries (HAGB) with trace inclination angles close to 90° relative to the tensile axis. DIC analysis further revealed that most GBs in the vicinity of the highly strained area cracked among random HAGBs with a high trace inclination angle to the tensile axis. This confirms that the local strain gradient at GBs plays an important role in SCC initiation, serving as a more suitable indicator of an additional stress component to effective normal stress acting on GBs compared to the Schmid factor mismatch.
Published Version
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