Improvement of the slurry erosion resistance of an austenitic stainless steel with combinations of surface treatments: Nitriding and TiN coating

Abstract

The combination of different surface treatments for improving the erosion resistance of an AISI 304 stainless steel was studied. Six kinds of sample conditions were tested in a slurry composed of distilled water and SiC particles: High temperature gas nitriding (HTGN), low temperature plasma nitriding (expanded austenite), high temperature gas nitriding followed by a PVD-TiN coating, low temperature plasma nitriding followed by a PVD-TiN coating as well as PVD-TiN coated and uncoated samples in the solubilized condition. The erosion tests were performed during 6 h in a jet-like device with a normal angle of incidence and an impact velocity of 8.0 m/s. Wear rates were assessed by accumulated mass loss measurements and through analysis of scanning electron microscopy images of the worn surfaces. The results were related to the microstructure and hardness of the surface to establish a ranking of the different surface treatments. After the first few minutes of testing cutting of the surface occurred in the solubilized, in the HTGN and in the low temperature plasma nitrided AISI 304 samples, whereas TiN coated samples did not show any cutting marks, although some indentation marks could be observed. The TiN coated samples showed wear resistances one order of magnitude greater than the solubilized, HTGN and low plasma nitrided samples.