Abstract

A special type of lead dioxide anode was found to be the most suitable anode material to produce iodate from iodide, periodic acid from iodine, and also to regenerate periodic acid (periodate) from iodic acid (iodate). This anode could be used in the absence of sulfate with a very slight loss. The yields of the products were almost quantitative with good current efficiency. Improved processes for the production of periodic acid from iodine and iodate from iodide using this anode and also those concerning the regeneration of periodic acid (periodate) from iodic acid (iodate) are covered in this paper.

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